GCMS results log, sample AD26991, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

- Data File C:\HPCHEM\1\DATA\DEC0 6 01\26991.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Heptadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.81 1.02 ng/uL 295236 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# %)

1 Heptadecane 240 C17H36 000629-78-7 (90/ 2 Pentacosane 352 C25H52 000629-99-2 87 3 Tricosane 324 C23H48 000638-67-5 87 4 Eicosane 282 C20H42 000112-95-8 87 Abundance Scan 2941 (31.809 min): 26991.D (-) m/ z 57.1.0 100.00% 57

5000 85 4 i ■ ■ ■ ■ i ■ TIIBP-C—OTT 99 31.40 31.60 31.80 32.00 32.20 A127........................... ' 1 P 1 1 ' 1 1 1>Ip >III II II P II II I I II II III IIII II«I IIII I<III I III I''’’I m/z 43.1.0 74.81% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71193: Heptadecane 57

5000 85 31.40 31.60 31.80 32.00 32.20 99 m/z 71.05 57.54% — J . 127141 169 210 240 IUPIPTITTTT I 1111j‘ ‘‘*P1 p • • • p • ’ ’ p • •' p ' • • l m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #49559: Pentacosane 43 57 TEI‘1 A ■ ■ i ■ ■ 31.40 31.60 31.80 32.00 32.20 5000- ' 85 m/z 85.05 42.08%

99 127 197 225 253267 325 352 0- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #46165: Tricosane — A —....... 43 57 31.40 31,60 31.80 32.00 32.20 m/z 55.10 25.46% 5000 85

m/z-> _ I 1' nI | 99 , 127 111'1,1 40 60 155 163 211 253 1 i । i i 1.1 [ > rP j .A. . । . . P । .7. . 0 . > > । > ri . । । । ^ p ii TTT 80 100 120 140 160 180 200 220 240 260 280 300 320 340 297 324 TTTII’r’i s ... I ! I ' ' ' ' I ' 31.40 31.60 31.80 32.00 32.20 YM. 26991.D NP112701.M Tue Dec 11 14:54:30 2001 Page 6

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