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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032421
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heptadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.81 1.45 ng/uL 525178 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS#

1 Heptadecane 240 C17H36 000629-78- 87 2 Eicosane 282 C20H42 000112-95- 87/ 3 Heneicosane 296 C21H44 • 000629-94-7 86 4 Dodecane, 1-iodo-___________________ 296 C12H25I 004292-19-7 86 Abundance Scan 2941 (31.808 min): 26986.D (-) m/z 57.10 100.00% 57 43 71 5000 85

99 113 127 141 155 207 ____________ 31.40 31.60 31.80 32.00 32.20 TI —l f T — i- 1— —I—I—I—I—I—I—1—TT—I—I—PITT r I T TTTTTr—I I y 1 TT m/z 43.10 67.05% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 57

71 5000 - 85 MT i ' ' 31.40 31.60 31.80 32.00 32.20

99 m/ Z 71" 05 62.35% J 113 127 141 155 169 210 240 । II— TITT ' ’ > i -r-r-n-p- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance

5000- 43 57

71 #72326: Eicosane

I." .A ■'I1 ' 31.40 31.60 31.80 32.00 32.20 m/z 85.1.0 40.76% 85

99 [ 1 • 113 127 141 155 J69 282 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72684: Heneicosane 43 5.7 31.40 31.60 31.80 32.00 32.20 m/z 41.10 23.84% 71 5000 85

22113 127 155 169 183 197 211 _ _ 269—296 / ■ • i > ■ ■ 11. ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00 32.20

26986.D NP112701.M Tue Dec 11 14:51:43 2001 Page 13

NYC-WTC_000032421

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NYC-WTC_000032421Source: NYC Law Department, mirrored locally

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