GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Octadecanoic acid, 2-methylpro Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.72 1.26 ng/uL 456975 Chrysene-dl2 33.19

Hit# of 5 Tentative ID, MW MolForm CAS# Qual

1 Octadecanoic acid, :2-methylpropyl e 34 0 C22H4402 000646-13-9 48 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11N02 040482-05-1 46 3 Cyclopentanecarboxylie acid, 2-amin 129 C6H11NO2 037910-65-9 43 4 Pentadecane, 8 -methyl ene- 224 C16H32 055668-09-2 38 Abundance Scan 2931 (31.716 min): 26986.D (-) m/z 56.10 100.00% 56

5000 41 73 I / TT । ।

miz-> 20 । ■ ■.1 p ■ 40 60 L21111. 97 129 TIWPpurr 185 267 285 241 “? | * 340 T 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00 m/z 57.10 55.55% Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 285 N I 1 ’ 1 ' I 31.40 31.60 31.80 32.00 m/z 43.10 46.27% 73 267 1 97 129 I I. . I 185 241 | 340 11' r ■ ■' ।1 • ■ ■ । ■ ■ ■ ■ ।'' ■' । TTTTTT • > < I 11''11111 1111 'l I I' • ■' I — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #5212: Cyclopenianecarboxylic acid, 2-amino-. trans- 56 T-r-j-r-r-r-r-j-r TTT 31.40 31.60 31.80 32.00 5000- m/z 41.10 39.76%

30 82 100 129 It I' • • •I''111 • ••. 11 I________________ ym-rTIT"II ‘TTT‘TIT‘r11IT T i ‘ ' i' " ■ i i ■ " ' i " '' i' ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- TI"L5m I 56 31.40 31.60 31.80 32.00 m/z 55.10 34.66% 5000

30 82 100 129 I'''' i'' 44 |,l, ,,, , ....... — —.. — — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

26986.D NP112701.M Tue Dec 11 14:51:41 2001 Page 12

NYC-WTC_000032420

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000032420Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS results log, sample AD26833, Dec 11 2001 · Box DEP Box 21

NYC-WTC_000032286

Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.998