GCMS results log, sample AD26988, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26988.D vial: 15 Acq On 6 Dec 2001 10:54 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\.1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.59 0.57 ng/uL 169105 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 32 2 2 -Methyl-N-1-tridecene 196 C14H28 018094-01-4 25 3 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 25 4 2-Methyl-1-Xetradecene 210 C15H30 000000-00-0 25 Abundance Scan 2699 (29.592 min): 26988.D (-) m/ z 56.10 100.00% 56

5000 43 73 257 T 116129 29.20 29.40 29.60 29.80 30.00 i ■ ■ • ■ । ■ ■ 117 TT101TTTTTT । 213 239 | • i > ■ ■ ■ i ■ • ■ ■ i > ■ ■ ■ i > ■ • • i ■ 312 TTTTTT m/ Z 57.1.0 52.14% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans­ 56

5000- ■ i ■ > ■ ■ i 29.20 29.40 29.60 29.80 30.00 ■ ■ A m/z 43.10 38.30% 30 69 82 100 129 ,l . . ii | !_____ _ 1 _ ____________ ; | ' ' ' ' I ' ■ ।1 ■ ■" 1 ■ l ■ ■ ■ ■ i • ■ • • । ■ • ■ ■ । ■ i • • ■ ■ । • i ■ • > ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21975: 2-Methyl-N-1-tridecene 56

29.20 29.40 29.60 29.80 30.00 5000 m/z 41. 35.96%

27 42 70 83 o i , 111 125 140 168181 196 IT ‘b1 1 I ’' ’ ’ I ' i • • • > ।' *»• । I » . > . ( . . > I| I I ! I | 1 i I I ]I I I I ! , I I q

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- I ___ ______ 56 ■ i ' ■ ■ • i 29.20 29.40 29.60 29.80 30.00 ' ' ' ' I ' ' ' ' I ' ' " ' I ' '

41 m/z 55. 0 32.23% 5000 73

i' ■r' i ■ ■ 1 113128 I •1,11• • • • i • • • • i' • • • i •'1 ' i 11... । .i । . 11।।। TIT ‘ ■ I 1 ■ ' ' i ' ' 1 i ■ ' ' ' i ' ' V N m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

26988.D NP112701.M Tue Dec 11 14:53:38 2001 Page 3

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