GCMS analysis results for sample AD26006, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentanecarboxylic acid, 2 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.56 1.13 ng/uL 366067 Chrysene-dl2 33.17

Hit# of 5 Tentative/ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 38 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 38 3 Oxirane, 2,3-bisk1-methylethyl)-, t 128 C8H160 054644-32-5 37 4 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 35 Abundance 7Scan 2695 (29.559 min): 26006A.D (-) ~ m/z 56.10 100.00%! 55

5000 43 73 ----- + A . । । । . 129 257 29.20 29.40 29.60 29.80 TT —11lH — 116 | 143157171 185 97 — 213 i • . 239 I • i • ’ ■ ■ i ■ • ' 1 । • 312 i ■ ■ ■ • i ■ ■ ‘ ■ i m/z 57.10 47.36% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- 56

5000- ‘i 29.20 29.40 29.60 29.80 30 m/ z 43.10 41.20% 69 82 100 129 .1 i'' ■ ■ |1 . J .1____ 1_______ ,RTIt ' • । < 1 *1 । i1,1 । I' '1 ’ I T' ‘ ‘ 1 i *' 1' i m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 56 #5212: Cyclopentanecarboxylic acid. 2-amino-. trans-

TT U 29.20 29.40 29.60 29.80 IT

5000 m/z 41.10 37.61% -

30 69 82 100 129 I । T l • • • • l ■ ■ ' • I I’।»>' • ।11'11 । ri-ri । i i i । । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- ‘T Tit

41 56 m/ z 29.20 29.40 29.60 29.80 55.10 30.73% 5000 73

m/z-> 20 i ■' ■ ■ i'' 40 60 ij| ।' .1. ।।।11.. 11 80 113 128 r1MI 100 120 140 160 180 200 220 240 260 280 300 —VL A 29.20 29.40 29.60 29.80

26006A.D NP112701.M Thu Dec 20 10:39:47 2001 Page 2

NYC-WTC_000030845

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