GCMS analysis results for sample AD26006, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Octadecanoic acid, butyl ester Concentration Rank 3

R.T. EstConc Area Relative to ISTD 4 R.T.

31.69 0.70 ng/uL 225280 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic acid, butyl ester 340 C22H4402 000123-95-5 (80) 2 1-Hexene, 2 -/nethyl - 98 C7H14 006094-02-6 35 3 Undecane, 5-methylene- 168 C12H24 005698-48-6 25 4 2 -Methyl- -tetradecene 210 C15H30 000000-00-0 25 'Abundance 7 Scan 2927 (31.686 min): 26006A.D (-) m/ z 56.10 100.00%| 56

5000 41 73 r . r ---—Ann = r 129 9AR

1 m/z--> 20 “ LL 40__ 60__ 80 1 . ...... . ....... ti"rrii 26725 .... To m/z "I‘‘-r‘TTI‘‘TTr‘t‘"T——rrtr‘ T’ItTrT I I |T 100 120 140 160 180 200 220 240 260 280 300 320 340 340 31.40 31.60 31.80 32.00 57.10 53.21% Abundance #73570: Octadecanoic acid, butyl ester 50

5000 285 340 31.40 31.60 31.80 32.00 73 129 267 m/z 43.10 45. 86% ।

m/z-> 20 i••i' 40 60 ! , 97 li. 1.1 I" r 11,111 •.. 185 11 '. ' ' I''' ' I '' ‘. I''' r '111 241 __I 11′1 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #1354: 1-Hexene, 2-methyl- I 56

41 31.40 31.60 31.80 32.00 5000 l m/z 41.10 38.97%- 1

| 83 98 TTppngn I r ■111 II... 11.... I ‘ TTT 11111 T‘"TTTETTF‘TTIT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #14771: Undecane, 5-methylene- 1 1 i ' I 56 ■ i ’ ■ 31.40 31.60 31.80 32.00 1 m/z 55.10 38.40%| 5000

27 | 83 । ‘O‘। ‘E10T — 111126 T‘TC 168 111" ■' i11 ■ ■ i ■ ■ ■■ i1"111111 rr'1111TTTT 1 i •• "| • 'T' ■ • • i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

26006A.D NP112701.M Thu Dec 20 10:39:49 2001 Page 3

NYC-WTC_000030846

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