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GCMS analysis results for sample AD26006, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030847
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Nonadecane, 9-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.78 0.55 ng/uL 176982 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane, 9-methyl- 282 C20H42 013287-24-6 2 Tetracosane 338 C24H50 000646-31-1 87 3 Docosane 310 C22H46 000629-97-0 86 4 Undecane, 2,3-dimethyl- 184 C13H28 017312-77-5 86 'Abundance Scan 2937 (31.778 min): 26006A.D (-) m/ z 57.10 100.00% 57 43 71 1 5000 85

99 Td IE1 . ................... ......... ............. 31.40 31.60 31.80 32.00 32.20 I — m/ z 43.10 67.22% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

N_ Abundance #39865: Nonadecane, 9-methyl- i !57 i i 71 I 85 i 5000 ‘ I ‘ ' ’“ I ' 1 ‘ 1 31.40 31.60 31.80 32.00 32.20 140 m/z 71.15 61.10% | 113. 99 168 ' 1 1 ’ ‘ TIT I . A * 111111 T' ' ' ' I 252 282 ' 1 ' 1 11''I 11 T‘ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73513: Tetracosane 43 57 71 144044.4 bom=paseq 31.40 31.60 31.80 32.00 32.20 5000 85 m/z 85.15 47.99%- 99 113127 155169183197 294 338 ■ i > • ■' i ■ ■ ■ ■ i ■ > ■ • i ■ • ■ > i • > ■ ■ i > • • ■ i • • > ■ i ■ ■ ■ > I > 1 11111 11 l1' ■ • I ’ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #44318: Docosane _W u • ( • r 1 T1 --A । 57 31.40 31.60 31.80 32.00 32.20 71 m/ z 41.10 2 9.07%| 85 5000

99 119 141155169,. . .. 266—. 310. . miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00 32.20

26006A.D NP112701.M Thu Dec 20 10:39:51 2001 Page 4

NYC-WTC_000030847

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