GCMS analysis results for sample AD26679, Dec 10 2001

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Library Search Compound Report

Data File C: \HPCHEM\1\DATA\DEC0401\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Nonadecane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.79 1.27 ng/uL 269486 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Nonadecane 268 C19H40 000629-92-5.87 2 Pentadecane 212 C15H32 000629-62-9 86 3 Eicosane 282 C20H42 000112-95-8 83 4 Hexatriacontane_____________ _ _______ 507 C36H74 000630-06-8 72 Abundance Scan 2939 (31.791 min): 26679.D (-) m/z 57.05 100.00% 57

43 71 5000 85

99 113 127 140 N I 11 ' 1 31.40 31.60 31.80 32.00 32.20 TIT

JUI +4 I ' ' 1 1 I — ■ f' ......... 207 ............... m/z 43.05 65.42% m/z-> 40 (60 80 100 120 140 160 180 200 220 240 260 280 [Abundance #37469: Nonadecane 57 43 71

5000 85 TT N ■ ■

31.40 31.60 31.80 32.00 32.20 i ■ •

m/z 71.05 54.27% 99 I ‘ 1 I ' 1 ' 1 r» ' • ' I 1 1 113 127 183 197 ...... 268. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #70278: Pentadecane 43 57 TI A I1'*’ 1 71 31.40 31.60 31.80 32.00 32.20 5000 - 85 m/z 85.05 41.16%

99 113 127 141 155 169 212 ' 1 i ' ■ ' r i 1 1 1 1 i ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane - 43 57 31.40 31.60 31.80 32.00 32.20 m/ z 41.05 24.69% 71 5000- 85

miz-> ‘It 40 |— — 60 80 . ................................ 99113120127 140 100 160 180 200 220 240 260 280 . -----................ .. . 31.40 31.60 31.80 32.00 32.20

26679.D NP112701.M Fri Dec 07 13:10:31 2001 Page 16

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