GCMS results log, sample AD27007, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Nonacosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

32.80 0.74 ng/uL 217517 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonacosane 408 C29H60 000630-03-5 2 Heptadecane 240 C17H36 000629-78-7 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 4 Tetracosane 338 C24H50 000646-31-1 87

1 Abundance ' Scan 3049 (32.801 min): 27007.D (-) m/ z 57.10 100.00% 57

5000 85 ---------------- b 113141 i ■ ' 1 ■ i ' 32.40 32.60 32.80 33.00 33.20 T’207 T) TTTTTTTTT I • I • 111 < 111 I' •' • I m/ Z 43.10 64.67% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane 43

71 5000 TT —IA 32.40 32.60 32.80 33.00 33.20 m/z 71.05 51.86% 29 127 211 239 379 408 TTTTT •' I'' i" • ■ i1"' i ■ " ' i ■"11" ■11" ■11" " i" " r " ' i" " I' I ’'' • I m/z-> 40 60 80 1 CD 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #71193: Heptadecane 5.7 -----AP — । 32.40 32.60 32.80 33.00 33.20 5000- 85 m/z 85.05 39.15%

| 113 , 141 169 210 240 r•*’i TUT]N—na TUUUuunn ———uunpumn Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 57 #42196: Heptadecane, 2.6,10,1 5-tetramethyl- .. --4 32.40 32.60 32.80 33.00 33.20 m/z 55.10 23.81% 5000 85

113 141 183 211 268 296 TT IT''' T ’ i'"' I" " i "1' i'' •' I'"11" ' ■ i" " i •"' i •' " i" " i' >" i" " i' •" t miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 32.40 32.60 32.80 33.00 33.20

27007.D NP112701.M Tue Dec 11 14:57:00 2001 Page 6

NYC-WTC_000032516