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GCMS results log, sample AD27007, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27007 completed on December 11, 2001.

NYC-WTC_000032503–000032519

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Hexatriacontane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.80 0.91 ng/uL 267119 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS#

1 Hexatriacontane 507 C36H74 000630-06-8 90 2 Eicosane 282 C20H42 000112-95-8 87 3 Eicosane 282 C20H42 000112-95-8 86 4 Octacosane 394 C28H58 000630-02-4 86 Abundance 57 Scan 2940 (31.802 min): 27007.D (-) m/z 57.10 100.00%| 43 71 5000 85 IL" ■ ■ i ■ •

ITt P— 1113,127.. ..... — 31.40 31.60 31.80 32.00 32.20 m/z 43.10 77.81% m/z--> 401 60 100 120 140 160 180 200 220 240 260 280 Abundance #74636: Hexatriacontane 43 57

71 5000 - Tt" TTP 85 31.40 31.60 31.80 32.00 32.20 m/z 71 • 05 62.15% 97 !m/z-> T"O"FECTEIETT 40 60 80 | 1 100 1 113 127 141 155 169 183 197 211 120 140 160 180 200 220 240 260 280 Abundance 472323: Eicosane 43 57 -4 —.... 71 31.40 31.60 31.80 32.00 32.20 5000 m/z 85.0 40.91% 85

99 113 127 141 282 n-1। ■ i , ' ‘ i ' 1 ' ' i 1 ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72326: Eicosane A i ' ■ ■ '

43 57 31.40 31.60 31.80 32.00 32.20 m/z 55.10 26.10% 71 5000 85 99 1 1 1 1 ' • 1 1 ' _ J,. 113 127 141 155 .............................. . i ' ' ' ' i ' ■ • l ■ A-- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.40 31.60 31.80 32.00 32.20

27007.D NP112701.M Tue Dec 11 14:56:57 2001 Page 5

NYC-WTC_000032515

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NYC-WTC_000032515Source: NYC Law Department, mirrored locally

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