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GC/MS analysis results for sample AD22558, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator; GALOS ■ Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Eicosane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

31.90 1.44 ng/uL 192046 Chrysene-dl2 ' 33.29

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Eicosane 282 C20H42 000112-95-8 91 Pentacosane 352 C25H52 000629-99-2 90 3 Hexatriacontane 507 C36H74 000630-06-8 90 4 Dotriacontane 451 C32H66 000544-85-4 90 Abundance Scan 2951 (31.895 min): 22558.D (-) m/z 57710 100.00% 5|7 43 71

5000 85

99 31.60 31.80 32.00 32.20 1 I 1 I ■p 1.1 127 m/z 43710 72.53% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43

5000 71 85 ... 7.L.... m/z 31.60 31.80 32.00 32.20 71.05 68T33%

TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73718: Pentacosane 43 57

71 31,60 31.80 32.00 32.20 5000 m/z 85.05 40.85% 85

, ,ll, l| , , T 169 183 197 211 225........................ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #74636: Hexatriacontane ..................................................... 43 5(7 31.60 31.80 32.00 32.20 m/z 41.10 26.05% 71 5000 85

97 I "I* , , i'* V, tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.60 31.80 32.00 32.20

22558.D NP072501.M Mon Oct 01 14:52:34 2001 Page 10.

NYC-WTC_000087114

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NYC-WTC_000087114Source: NYC Law Department, mirrored locally

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