GC/MS analysis results for sample AD22558, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS ■ Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DAT7kBASE\NBS75K.L ************************************************************************** Peak Number 9 Octadecanoic acid Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 31.80 0.62 ng/uL 82868 Chrysene-dl2 ' 33.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octad^anoic acid 284 C18H36O2 000057-11-4 27 2 2-ChWro-2-methylnonane 176 C10H21C1 004325-50-2 25 3 Pen^decane, 8-methylene- 224 C16H32 055668-09-2 25 4 l-yhdecene, 10-methyl- 168 C12H24 022370-55-4 23 ^bundanofe Scan 2941 (31.804 min); 22558.D (-) Tin/z 56.10 100.00% 5|5

5000 43 73 85 101 116”'?® 285 31.40 31.60 31.80 32.00 32.20 II m/z 57.10 61.31% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72362; Octadecanoic acid 5Z 73

5000 T' ' ' ' I ' ' ' ' I ' “ ‘ ' I ' ' 31.40 31.60 31,80 32.00 32.20 «%7 129 m/z 43.10 45.08% 284 241 I I I A ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ^bundance #16689; 2-Chloro-2-methylnonane 55 69 31.40 31.60 31.80 32.00 32.20 5000 m/z 41.10 43.86%

35 I 7 97 112125 ^1° 11'' I ’ ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ‘ ' t n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #28775; Pentadecane, 8-methylene- 31.^ 31.60 31.80 32.00 32.20 m/z 55.10 . 35741%

5000 69

27 I, V 112125 140 j L •yrV- iH III II J I 4 —T- 196 _224 ' ’ 1' ''' I'' P * ' ' I ' ‘ ' I Tl/Z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31.40 31.60 31.80 32.00 32.20

22558.D NP072501.M Mon Oct 01 14:52:31 2001 Page 9

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