GC/MS analysis results for sample AD22558, Oct 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GTkLOS . Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heptadecane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.87 0.52 ng/uL 69313 Chrysene-dl2 - 33.29

a Hit# of 5 Tentative ID MW MolForm CAS# Qual

Heptadecane 240 C17H36 000629-78-7 83 Hexadecane 226 C16H34 000544-76-3 53 3 Hexane, 2,2,3,3 -tetramethyl- 142 C10H22 013475-81-5 50 4 Heptane, 2,2,3,3,5,6,6-heptamethyl- 198 C14H3 0 007225-67-4 42 Abundance Scan 2839 (30.868 min): 22558.D (-) m/z 57710 100.00% 57 A 43 71

A 5000 85

30.60 30.80 31.00 31.20 , , III, , , l|l , , ll.......... .................. .......... m/z 43.10 7^777% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 57 43

5000- 71

85 A A T-r-p-r 30.60 30.80 31.00 31.20 m/z 71.05 62.76% .''r^ ....................................................... nn/z-> 40 I60 80 100 120 140 160 180 200 220 240 Abundance #70789: Hexadecane 57 43 ' ' I '' '' I 30.60 30.80 31.00 31.20 71 m/z 85.05 40.43% 5000 85 A

■n/z-> Abundance 40

43 . 57 ' I ' ' 60 80 100 ^13 1^.................... ^6 120 140 160 180 #8106: Hexane, 2,2,3,3-tetramethyl- 200 220 240 n 30.60 30.80 31.00 31.20 m/z 41.10 28770% A 5000- 85

71 99 TT—f-r-r ,,, ll, , ' I ' ' ' ' I I J.............. ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20

22558.D NP072501.M Mon Oct 01 14:52:29 2001 Page 8

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