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GC/MS analysis results for sample AD23261, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23261 conducted on October 12, 2001.

NYC-WTC_000088098–000088114

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088111
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23261.D vial: 7 Acq On 9 Oct 2001 7:13 pm Operator: 2 09 GALOS, Sample g c/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heptadecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.61 0.51 ug/1 95077 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 96v 2 Octadecane 254 C18H38 000593-45-3 95 \ 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1. 91 / 4 Heneicosane 296 C21H44 000629-94-7 9/ Abundance Scan 3221 (34.614 min): 23261.D {-) “m/z 57700 100.00% 57

85 5000 4' Hl 1 ''i^ ■‘*1 169 221 240256 34.20 34.40 34.60 34.80 35.00 '’ T'' -T-fT-TTT^-TTT+p-rT-IJ-rT-I-rjTT-I-IJTTT-q^^ "m/z 71.10 67.62% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 57

85 553 34.20 34.40 34.60 34.80 35.00 m/z 43.00 62.25% ' ' I ' ' I'' I''' 'I'' f' I " ” I' " ’ I " '' I" '' I" " I' "' I " '' I'''' I'' " I'" ’ I ” ’' I'''' I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane 5(7

I' ' ' n ' ' 34.y 34.40 34.60 34.80 35.00 5000 85 "m/z 85.05 51.26%

,,l j I 141 169 197^ 254 m/z-> Abundance 40 60

57 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #49558: Heptadecane, 9-octyl- H I' 34.20 34.40 34.60 34.80 35.00 m/z 41705 27.60% 5000 85

..... T 31.0 352 I'''' I f’ I'''' I'' " I' " ' I " '' I'' " I'' " I' " ' I " '' I'''' I " " I' " ' I " '' I'' " I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23261.D NP091101.M Thu Oct 11 10:45:59 2001 Page 7

NYC-WTC_000088111

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NYC-WTC_000088111Source: NYC Law Department, mirrored locally

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