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GC/MS analysis results for sample AD23261, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23261 conducted on October 12, 2001.

NYC-WTC_000088098–000088114

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088110
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT0901\23261.D Vial: 7 Acq On : 9 Oct 2001 7:13 pm Operator: 209 GALOS Sample : g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Hexatriacontane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.69 0.64 ug/1 119167 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Tetracosane 338 C24H50 000646-31-1 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Nonacosane ____________________ 408 C29H60 000630-03-5 91 Abundance Scan 3120 (33.687 min): 23261 .D (-) m/z SYTOO 100.00% 57 71 43 85 5000

33.40 33.60 33.80 34.00 m/z 71.00 75.85% TT/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

253 71 85 A A 33.40 33.60 33.80 34.00 m/z 43.05 70.01% I I T ,12’' 27141155169183197211 I ' ' ‘ ' I ' ' r ' ' I ' ' '' I ‘ ' r ' ' ' I ' ' ' ' I ' ' ' ' I I ' ' ' ' I ‘ ' I' ' ' ' I ' ' ' ' I ' ' ' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 33.40 33.60 33.80 34.00 5000- 85 m/z 85.05 54.06%

I II || \|'^127 155169183197 294 338 p-TVq^hnnYTT-VTpVrp-T-rT^qT-lHnyVrTTp-TTpnT-TTp-rTTpT-T^^ I' '' 'I' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #73718: Pentacosane / 4(3 5,7 33.40 33.60 33.80 34.00 m/z 41705 25.72% 71 5000 85

I ^^113127141155169183197211225 -q-nr-r-q-r p-rr-q-TT-rq- I ' ' ' ' I ' '‘ ‘ I ' ' ' ' I ' ' ' ' I ' ‘ ' I •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

23261.D NP091101.M Thu Oct 11 10:45:56 2001 Page 6

NYC-WTC_000088110

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NYC-WTC_000088110Source: NYC Law Department, mirrored locally

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