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GC/MS analysis results for sample AD23125, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23125 conducted on October 12, 2001.

NYC-WTC_000088023–000088043

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088037
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT04 01\23125.D Vial: 13 Acq On 5 Oct 2001 3:16 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Hexatriacontane Concentration-Rank 4

R.T. EstConc Area Relative to ISTD R.T.

32.76 1.33 ug/1 263649 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91\ 2 Octadecane 254 C18H38 000593-45-3 91 3 Nonacosane 408 C29H60 000630-03-5 91 4 Pentacosane 352 C25H52 000629-99-2 91 Wjundance Scan 3019 (32.756 min): 23125.D (-) m/z 57.0,0 100.00% 57 A

5000 85

, i li 11 J J 141 169 211 253 281 32.40 32.60 32.80 33.00 352 p''' p • i|' 'Ti I n 11 y 1111J 'i f I I’jTi I f I'l 11111111111111J11111J m-rr pTrrp-rrrj m/z 71.00 67.92% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #74636: Hexatriacontane i . 57

5000 85 32.40 32.60 32.80 33.00 m/z 43.05 64.13% I 1 U ”',(5 , 141 169 197 hi/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #71561: Octadecane 5/ T 32.40 32.60 32.80 33.00 85 5000 m/z 85.0,5 46.28%

224 254 JTTTtprrrpTTTYTTTTJ^^ 1.11 I, I. I I J i l l rp 1111 pTTTTTTrrj-rrrrr 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane I 43 32.40 32.60 32.80 33.00 m/z 41.05 25.26% 71 fl 5000

J11 n 11 r I.. IF. I. j. I r I 211 239 ''''I'"'i'' 379 408 ‘' I ’ " ' I' " ' m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 32.40 32.60 32.80 33.00

23125.D NP091101.M Tue Oct 09 12:44:05 2001 Page 8

NYC-WTC_000088037

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NYC-WTC_000088037Source: NYC Law Department, mirrored locally

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