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GC/MS analysis results for sample AD23605, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23605 conducted on October 19, 2001.

NYC-WTC_000088935–000088960

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088953
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23605.D Vial: 12 Acq On : 17 Oct 2001 1:00 am. Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexatriacontane Concentration Rank 1. R.T. EstConc Area Relative to ISTD R.T. 33.69 2.63 ug/1 279584 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 9L 2 Docosane 310 C22H46 000629-97-0 91 3 Nonacosane 408 C29H60 000630-03-5 93/ 4 Pentacosane 352 C25H52 000629-99-2 90 Wjundance Scan 3121 (33.694 min): 23605.D (-) m/z 57.00 100.00%

5000- 85

........ )........... I I J J ■’69.197 239 281 33.40 33.60 33.80 34.00 ' I ‘ ” ' ' * * ' ' ' I ' ' ' ’i ' ' -' ' I ' m/z 71.10 7^/07% iiZz-> 50 100 150 200 250 300 350 400 450 500 flibundance #59136: Hexatriacontane 7

5000 85 33.40 33.60 33.80 34.00 m/z 43.05 62.84% 113 141 i| 239 379 407 435 478 506 ' ' I ' ' ' ' I ' Ti/z-> 50 150 200 250 300 350 400 450 500 Abundance #44318: Docosane ' ^'1 7 1 I > I r . ^1 r I fl 1'1 I- i-r- 57

85 33.40 33,60 33.80 34.00 5000 m/z 8^705 49731%

|113 44,4 J.lj ...... 266, , 3’0 .......... . , , nZz-> Abundance 50 43 100 150 200 250 300 #54526: Nonacosane 350 400 450 500 A . 33,40 33.60 33,80 34.00 ..m/-z— 41.05 ' ' I ' '

22.70% 71 5000

. . I f . r f 211^9 .......... 379 408......... ' ' I ' ■nfe-> 50 100 150 200 250 300 350 400 450 500 33.40 33.60 33.80 34.00

23605.D NP091101.M Thu- Oct 18 10:32:45 2001 Page 12

NYC-WTC_000088953

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NYC-WTC_000088953Source: NYC Law Department, mirrored locally

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