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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086967
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546 .D vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.64 1.10 ug/1 168479 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91s 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tricosane 324 C23H48 000638-67-5 91 4 Nonacosane 408 C29H60 000630-03-5 91 ’ Abundance Scan 3224 (34,638 min); 22546. D (-) m/z 57.00 100.00% 57 71 43 85 5000

^bundance XU40 60 .i Jj 113 J T'lf 155169183197211225 T‘TTT-tYrr^rp‘VrT-|H-TTVp-l‘TT7-rT-rTYr-rTTpT-rTyrT^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 #74636: Hexatriacontane 255 m/z 34,40 34,60 34,80 35,00 71.10 69.83%

43 57

71 5000 85 34,40 34,60 34,80 35,00 m/z 43.00 62.72% I T 155169183197211 ' ' I ’ IT11 . j 11 r 111 t»11* 111 'i Y11111 *«< 1111111 I ' ' ' ' I ' ' ' ' I ' ' ' ' I p-T 7i/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 57 71 T 85 34,40 34,60 34,80 35,00 5000 m/z 85.05 49.49% 99

.1... .... ..................... ???■,■,???....... Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 3 5|7 34,40 34,60 34,80 35,00 m/z 55.00 24.11%

5000 71 85 J

■nfe-> J t __________ 296 3^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 34,40 34,60 34,80 35,00

22546.D NP091101.M Wed Oct 03 14:44:46 2001 Page 11

NYC-WTC_000086967

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NYC-WTC_000086967Source: NYC Law Department, mirrored locally

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