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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 Acq On : 2 Oct 2001 4:04 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.71 1.27 ug/1 191421 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qnal

jMlexatriacontane 507 C36H74 000630-06-8 94 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tricosane 324 C23H48 000638-67-5 91. 4 Tritetracontane 605 C43H88 007098-21-7 91 <\bundance Scan 3123 (33.714 min): 22913.D (-) m/z SYTOO 100.00% 57 71 43 5000 85

I 99 J T 33.40 33.60 33.80 34.00 I I II j J, .iJ ^r^Fl?1155169183197211 227 253 I I p I iT| I n I I " I 1 I j I I T I I I I I 11. I I 'i I I f I I I ’l 1 i I I I i I I I I I I ■l " '' I p-rT-T-p-TTTT m/z 71.00 76769% tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ^bundance #74636: Hexatriacontane 43 5l7

71 5000 85 33.40 33.60 33.80 34.00 m/z 43.00 65.49% 99 I T I 1 I J I I rr I I I I I i' I I I ’• I I I I I I I 1 I I I I i I I ■p-TTTT nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 5|7 71 85 33.40 33.60 33.80 34.00 553 m/z 85.05 48.87% 99 268 296 r ' ’' r ''' I '''' I Tl i i-rpnn l p n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane y T"^ 43 57 33.40 33.60 33.80 34.00 m/z 41.05 26737% 71 5000 85

■nZz-> XU 40 60 I n-i-. J11 f l 111.1 0- 80 183197211225 I ' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 320 I' * ' * I 296 324 ''' I * * * * I *'' 33.40 33.60 33.80 34.00

22913.D NP091101.M Wed Oct 03 09:31:18 2001 Page 10

NYC-WTC_000087533

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NYC-WTC_000087533Source: NYC Law Department, mirrored locally

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