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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexacosane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.72 1.55 ug/1 238402 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual (^Hexacosane 366 C26H54 000630-01-3 95 2 Eicosane 282 C20H42 000112-95-8 93 3 Tetracosane 338 C24H50 000646-31-1 91 4 Octadecane 254 C18H38 000593-45-3 91 Abundance Scan 3124 (33.720 min): 22546.D (-) Wz 5^/95 100700% 57

85 5000

Ui .1, ll J 197 227 253 282 366 • q " " I ' ‘ ” I r. . I 33.40 33.60 33.80 34.00 m/z 71.00 77757% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73943: Hexacosane 57

55S 85 33.40 33.60 33.80 34.00 m/z 43705 68.27% , __________ 339 366 nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72326: Eicosane 57

^.40 33,60 33.80 34.00 50CX) m/z 85.05 57.76% 85

» 282 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73543: Tetracosane 57 33.40 33.60 33.80 34.00 m/z 55.00 26.11% 5000 85 ft Ti/z--> I I 113 It./.. 155 183 ' H ' T" ' 294 -m-j- 338 . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 4 33,40 33,60 33.80 34.00

22546.D NP091101.M Wed Oct 03 14:44:44 2001 Page 10

NYC-WTC_000086966

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NYC-WTC_000086966Source: NYC Law Department, mirrored locally

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