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GC/MS analysis results for sample AD22977, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22977 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087731–000087753

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0 3 01\22977.D Vial: 3 Acq On 3 Oct 2001 2:36 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexatriacontane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

35.53 0.84 ug/1 96003 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91, 2 Nonacosane 408 C29H60 000630-03-5 90 3 Triacontane 422 C30H62 000638-68-6 90 4 Docosane 310 C22H46 000629-97-0 90 lAbundance Scan 3321 (35.525 min)? 22977.D (-)' m/z~57 70,0 “lOO". 00% 57

I 85 5000 [ 35.20 35.40 35.60 35.80 m/z 71.10 70.37% m/z-> 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #74636; Hexatriacontane 7

5000 85 ' 'T' rc.i . 35.20 35.40 35.60 35.80 m/z 43.05 63.17% U '’P , 141 169 197 . iT. j I . . . i'. . . I I . . , . I , , . 1 I . I' ‘ " I " ’' I I" " I" " I 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #54525: Nonacosane «]

: 71 35.20 35.40 35.60 35.80 5000 m/z 85.05 50.49% i i A 211 239 379 408 ''" I ” " I''" I I" "1" ” I TTyrrnyrrn-f m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #55461: Triacontane 43 35.20 35.40 35.60 35.80 m/z 55.00 23.94% 71 5000

■m-p-TT Jj Tje 239 267 yrrnyrrny '' i" " I" " 379 422 " I" " I" " I"' 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 35.20 35.40 35.60 35.80

22977.D NP091101.M Tue Oct 09 09:49:01 2001 Page 12

NYC-WTC_000087749

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NYC-WTC_000087749Source: NYC Law Department, mirrored locally

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