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GC/MS analysis results for sample AD22979, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22979 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087773–000087793

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22979.D Vial: 5 Acq On 3 Oct 2001 4:33 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.52 0.84 ug/1 118043 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91\^ 3 Triacontane 422 C30H62 000638-68-6 91 / 4 Nonacosane 408 C29H60 000630-03-5 90/ Abundance Scan 3320 (35.522 min): 22979.D (-) m/z 57.0,0 100.00% 57

85 5000

35.20 35.40 35.60 35.80 m/z 70.9,5 70.62% 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380400 420 Abundance #74636: Hexatriacontane 5i7

5000 85 .................... 35.20 35.40 35.60 35.80 m/z 66.81% a I Il , 141 169 197 i | . il l I 11 I . | > H l I > r > , I I I , I , . . . , J . . , I I I ‘' I " " i I' ” ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 57

85 #42201: Heneicosane

T A I ' ' ' ‘ I 35.20 35.40 35.60 35.80 5m m/z 85.05 52.56%

113 ... I , I I’ ‘ "fI " '' I " " I ’ " ' _________ 268 296_______________ .. I" ' * " {' > " I " " I' * " I' " * I rnT|.. 111111. J111.1.1.11.11111111 I m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 'Abundance #55461: Triacontane P ■ ' ■ t I 43 -_312O_354O_J5,6O_^5,8^^ m/z 54.95 24.84%

m/z-> 52H 71

■" p" I. r.. IT. I q.. V. 11. i' 239 267 379 422 yrTTTpTTTpTTTpTTTT '' I" " I “ " I "' 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 420 1 35.20 35.40 35.60 35.80

22979.D NP091101.M Tue Oct 09 09:54:50 2001 Page 10

NYC-WTC_000087789

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NYC-WTC_000087789Source: NYC Law Department, mirrored locally

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