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GC/MS analysis results for sample AD23503, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.

NYC-WTC_000088905–000088934

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088925
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23503.D Vial: 11 Acq On : 17 Oct 2001 12:01 am Operator: 209 GALOS Sample- ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 35.50 1.74 ug/1 166224 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Triacontane 422 C30H62 000638-68-6 91 4 Eicosane, 7-hexyl-_____________ 366 C2-6H54 055333-99-8 91 Abundance Scan 3318 (35.505 min): 23503.D (-) m/z 57.00 100.00% 5)7

85 5000

Frpm-i-i f-r, , I 3520 35.40 35.60 35.80 281 p-rrrpT-rrjTTTTp-rTTp-rrrp-rTTp-rTTpT^^ m/z7171073.65% tt/z-> 40 60 80 100120140160180 200220 240260280 300320340360380 400420 Abundance #74636: Hexatriacontane 5|7

5000 , .-r, , p^,-. |-r . 85 35.20 35.40 35.60 35.80 m/z 43.05 69.39% J 11212141 169 197 • . TiZz-> 40 60 80 100120140160180 200220 240 260280 300320340360380 400420 Abundance #42201; Heneicosane _5t?’- p-rT-n 1 /, , , I I TTryn T7~| 85 35.20 35.40 35.60 35.80 253 m/z 85.05 49.90%

I 113 lyn ■m-p-rr 268 296 pTTn-pTTTp-rxTp-TTrpYTTynn-tyrTTTp-rrrpnnTyr^^ ■ . . _ . n/z-> 40 60 80 100120140160180 200220 240260280 300320340360380 400420 Abundance #55461; Triacontane ' ^1 " -r-r-p-r^-r-r-r-pV-5^-r-r-p--r-i-i-| 43 -^35.20-35.40-3560 35.80--::- -m/z- -55-. 00- 26vl6% 7,1 5000

239 267 379 422 A/V p/AM A/pz A I ‘" 111" ■ I" " I" " 1" I-1111" I nfe-> 40 60 80 100120140160180 200220 240260280 300320340 360380400420 35.20 35.40 35.60 35.80

23503.D NP091101.M Thu Oct 18 10:29:11 2001 Page 14

NYC-WTC_000088925

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NYC-WTC_000088925Source: NYC Law Department, mirrored locally

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