GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28693.D Vial: 8 Acq On 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 35.42 0.68 ug/1 102349 Perylene-dl2 37.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 2 Tritetracontane 605 C43H88 007098-21-7 0 3 Tetratetracontane 619 C44H90 007098-22-8 90 4 Heneicosane 296 C21H44 __ ______ 000629-94-7 87 Abundance Scan 3309 (35.420 min): 28693.D (-) m/z 57.00 100.00% 57

85 5000 MC-pAPA r r ( - T r — ( -- I l~

113141169 207 35.00 35.20 35.40 35.60 35.80 T L 1 — 4 — ill — I t I — -------------------- — ------------------- m/z 43.05 69.06% m/z-> 100 150 200 250 300 350 400 ' 450 " 500 " 550 " 600 ' 50 Abundance #74636: Hexatriacontane 57

5000 85 35.00 35.20 35.40 35.60 35.80 m/z 71.10 66.22%

m/z-> .L 50 113141169197 .......... . , , | ,,,,,, , 100 150 200 250 300 350 400 450 500 ‘ 550 600 Abundance #60913: Tritetracontane 57 A PP-A4 4 . — A 35.00 35.20 35,40 35.60 35.80 5000 85 m/z 85.05 50.86%

mz—> ■ • ■ i • 50 1’111 100 150 196 200 250 300 350 400 463491519547576604 450 500 550 600 Abundance #74745: Tetratetracontane 57 —A— 35.00 35.20 35.40 35.60 35.80 m/z 55.00 24.94% 5000- 85

. . ....................................... 463491519547,591618 m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 35.00 35.20 35.40 35.60 35.80

28693.D GCMS1126.M Thu Dec 06 15:19:54 2001 Page 10

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