GCMS analysis comments for sample AD28664, Dec 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

35.43 0.45 ug/1 80769 Perylene-dl2 37.13

Hit# of 5 Tentative ID MW MolForm CAS# 1

1 Hexatriacontane 507 C36H74 000630-06-8 (91 2 Tetratetracontane 619 C44H90 007098-22-8 87 3 Tritetracontane 605 C43H88 007098-21-7 87 4 Tridecane, 1-iodo- 310 C13H27I 035599-77-0 86 •Abundance .............. Scan 3310 (35.429 min): 28664.D (-) m/z 57.00 100.00% 57

5000 85 A 1P 1 4 - 4444 (113 155 191 35.00 35.20 35.40 35.60 35.80 1 ---mm — . . . । . . . .. I । । । । । । I । m/z 73.52% miz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000 85 11A 35.00 35.20 35.40 35.60 35.80 m/z 43.00 70.47% ■ ■ i ■ 1113141 169197 .................. miz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74745; T etratetracontane 57 A+-WPATSPR 35.00 35.20 35.40 35.60 35.80 5000 - 85 m/z 85.05 40.86%

. ................................. 463491 519547.591618 50__ 100 150 200 250 300 350 400 450 500 550 600 Abundance #60913: Tritetracontane -AAAne . 57 35.00 35.20 35.40 35.60 35.80 m/z 40.95 23.40% 5000 85

1 miz-> ■ ■ i ■ 50 111 141 196 — ‘IIEEEII_ 100 150 463491519547576604 ‘II1‘IID—EII01CCIT1"CLTII1LTIVIIT1I 200 250 300 350 400 450 500 550 600 Mnnl Mt 35.00 35.20 35.40 35.60 35.80

28664.D GCMS1126.M Fri Dec 07 15:54:24 2001 Page 10

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