GCMS analysis log for sample AD30696, Jan 2002

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Data File C:\HPCHEM\1\DATA\DEC3101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

38.24 1.10 ug/1 154738 Perylene-dl2 37.12

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Tritetracontane 605 C43H88 007098-21-7 91 4 Triacontane 422 C30H62 000638-68-6 87 Abundance 57 Scan 3616 (38.238 min): 30696.D (-) m/z 57.00 100.00%

5000 85

.................................. ........ ....... vaam 38.00 38.20 38.40 38.60 * TY m/z 43.05 81.92% miz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane

7 57

5000 85 38.00 38.20 38.40 38.60 m/z

miz-> ■1 r1 50 I‘ 100113141169 197 . ........ 150 ‘ 200 ‘ ' 250 ‘ 300 350 ' 400 450 500 550 600 Abundance #74745; Tetratetracontane 57 "II Tda 1111104s a 38.00 38.20 38.40 38.60 5000 85 m/z 85.05 46.93%

! : ; [ 113141 463491519547 591618 ’ i 1 • IIF4I1 1 ' 1 ‘l 1 1 ' ' I '■ ' m/z-> Abundance 50 • •»■ 1 • I ■ ■ 1 1 i • ‘ 1 ' i 1 ‘ 100 150 200 ■ i 1 ■ ‘ ■ i • ■ ■ • i 1 ‘ 250 300 350 #60913: Tritetracontane 400 450 500 550 600 57 38.00 38.20 38.40 38.60 _________ / m/z 41.05 2 9.93% 5000 85

* ■ i * .1,1113141 ., ..... ...... 463491 519547 576604 4* II*}* i । » I i r-j i 18* m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 38.00 38.20 38.40 38.60

30696.D GCMS1126.M Wed Jan 23 08:37:18 2002 Page 10

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