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GCMS analysis log for sample AD30696, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

NYC-WTC_000018123–000018141

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018138
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

36.27 2.86 ug/1 403635 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriaco; ane 507 C36H74 000630-06-8 94 2 Dotriaco ane 451 C32H66 000544-85-4 91 3 Tetrat racontane 619 C44H90 007098-22-8 91 4 Eico .ne, 7-hexyl- 366 C26H54 055333-99-8 91 • {Abundance Scan 3402 (36.273 min): 30696.D (-) m/z 57.00 1 00.00% 57

5000 85

36.00 36.20 36.40 36.60 TTtJ 1,113141169 197225252 281 .... m/z 43.05 82.98% miz-> 50I ioo 150 200 250 300 350 400 1450 500 550 ‘ 600 ‘ Abundance #74636: Hexatriacontane 57

5000 85 4 • ‘ I * * rj ‘ ‘ • • J ‘ 1 T 36.00 36.20 36.40 36.60 m/z 71.05 67.24% 1 111 113141150169197 Iioo ........................................... miz-> 50 ‘ ' 200 250 ‘ 300 350 400 ' ‘ 450 500 550 ' 600 ' Abundance #74491; Dotriacontane 57 T — T T 36.00 36.20 36.40 36.60 5000 85 m/z 85.00 45.70%

1 113141 196 281 422450 miz-> 50 100 150 200 250 300 350 400 ' 450 500 550 ' 600 Abundance 57 #74745: Tetratetracontane mm 2 , mmmmm 36.00 36.20 36.40 36.60 m/z 41.05 32.21% 5000 85

.. I 1113147.463491 519547 591618 50 ioo 150 ‘ 200 ‘ 250 ' ‘ 300 350 400 ' ' 450 500 ‘ ‘ 550' ‘ 600 ‘ m/z-> 36.00 36.20 36.40 36.60

30696.D GCMS1126.M Wed Jan 23 08:37:13 2002 Page 9

NYC-WTC_000018138

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NYC-WTC_000018138Source: NYC Law Department, mirrored locally

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