GCMS analysis results for sample AD31641, February 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN0302\31641.D Vial: 39 Acq On : 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample : gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 36.11 1.64 ug/1 174859 Perylene-dl2 36.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane 240 C17H36 000629-78-7 87 4 Nonadecane 268 C19H40 000629-92-5 87 Abundance Scan 3384 (36.108 min): 31641.D (-) m/z 57.00 100.00% 57 __

5000 85 fiT TTTerrf I J 1’13,141 169 209 TPI Rp"TT i»i f |‘i i i । i i i r । । i i' i [ r i i i । । i i । । i । i i [ ri ■ r । ■ 35.80 36.00 36.20 36.40 r m/z 43.05 73.86% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #59136: Hexatriacontane 57

5000 7 ‘ 1 1 ‘ • 1 I T T T 85 35.80 36.00 36.20 36.40

11 58.87%

m/z-> TI— 50 100 113141 150 239 ’*I**+I**’’I-I-IIIT ' 1 1 I 1 ' ' 1 !"• 1 200 250 300 350 400 450 500 379 407 435 478 506

Abundance #42201: Heneicosane 57 Tiinemmnifi 85 35.80 36.00 36.20 36.40 5000 m/z 85.0. 44.52%

। • • 113 .9// 141 . ................................. . , . miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #71193: Heptadecane --P-—T4A t 57 35.80 36.00 36.20 36.40 m/z 41.05 26.16% 5000 85

210 240। t i i i j ( I I I | I I | I | I r 1 4'1 " 3' I 1' f | 1 f 113,141 169» I jlii! »| «»i i | » k • ■ i ■ m/z-> 50 . 100 150 200 250 300 350 400 450 500 35.80 36.00 36.20 36.40 ' 1

31641.D GCMS1126.M Pri Feb 01 11:17:05 2002 Page 7 NYC-WTC_000049758