GCMS analysis results for sample AD31641, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JANO302\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample gems scan 1/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Pentatriacontane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 35.25 1.21 ug/1 129087 Perylene-dl2 36.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentatriacontane 2 Hexatriacontane 3 Dotriacontane /0, 493 C35H72 507 C36H74 451 C32H66 000630-07-9 000630-06-8 91 000544-85-4 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance Scan 3290 (35.245 mln): 31641.D (-) m/z 57.00 100.00% 57

5000 85 ftTAAr 35.00 35.20 35.40 35.60 39T 1433133155, 191,, '250' ‘300 350" 460' 1 ‘ '450' m/z 43.0 76.91% mlz-> 50 100 150 200 Abundance #58743: Pentatriacontane 57

5000 85 YYTT T T 35.00 35.20 35.40 35.60 m/z 71.00 63.91% ■ ■ i ‘ T . 1। 113,141 I , 225 *197 .169 " . 7 1“ BTTrt j i i "if miz-> 50 100 150 200 250 300 350 400 450 Abundance #74635: Hexatriacontane 57 35.00 35.20 35.40 35.60 5000 85 rn/z 85.05 .................... 40.90% ...........................

; ■1- 1 | l r i1 > 1 i1 i i i | 1 i 113 141 196 225 253 281 ■ • i ■ ■ ' 1 1 • • • 1 i ■ > I 4 » > > I I t 1 I" I I miz-> 50 100 150 200 250 300 350 400 450 Abundance #74490: Dotriacontane ‘ **I**‘I***I‘‘1UTS 43 35.00 35.20 35.40 35.60 m/z 41.00 31.81% 5000

m/z-> ■ • 50 i ■ 71

97 1,u . ......................... ............... 379 407 . 450 100 150 200 250 300 350 400 450 AAML X, f . . Y . । i ri i । > i i i । i i’i 35.00 35.20 35.40 35.60

31641.D GCMS1126.M Fri Feb 01 11:17:00 2002 Page 6

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