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GCMS analysis results for sample AD31641, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049756
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\ JAN0 302\31641.D Vial: 39 Acq On 4 Jan 2002 11:32 pm Operator: 209 GALOS Sanpl e gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Eicosane, 7-hexyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

34.36 0.44 ug/1 73093 Chrysene-dl2 32.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane, 7-hexyl- /0 . 366 C26H54 055333-99-8 91 2 Heptadecane , 9 - octyl - / 5. 352 C25H52 007225-64-1 90 3 Eicosane, 9-octyl- \ .y 394 C28H58 013475-77-9 86 4 Octacosane ________ Vy 394 C28H58 000630-02-4 86 Abundance / Scan 3194 (34.364 min): 31641 .D(-) m/z 57.0,0 100.00% 57

5000 85

m/z-> Abundance a4 155 TpR 207 253 281 TVIPWn—em—gunun98mBa—n———BapBmT m/z 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #50999: Eicosane, 7-hexyl- "NY? Mi 1rr TTPPYMMM r 34.00 34.20 34.40 34.60 43.00 82.21%

57

wAAMMMAM N, , ,TM AMA, 5000 85 34.00 34.20 34.40 34.60 ' m/ z 71.Q0 57.66% “ ’ 14 “ 111,141 1822813 1‘n00u1m551‘35110019B20901910099—1——BOBIBIEIDTD311113 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #49558: Heptadecane. 9-octyl- 57 "I" ’)• 34.00 34.20 34.40 34.60 5000 85 m/ Z 85.05 43.90%

| 13141169 ........ 239........ 310... 35202270333317 miz-> Abundance 2190m9330‘m20001102109221107mnn— naa222223900933302223233322932192 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 43 #53460: Eicosane, 9-octyl- 1 i ■ • A ■ ' i • • ■ • i • 34.00 34.20 34.40 34.60 m/z 41.Q5 28.57% 71 5000

1 99 197 . 238 281 m/z-> ‘"P" 1,127,155 TTnpmem —n—a—_____ 352 394 -18 —1—mpn"nmegDDTT mn—mmmpmmeEnmn 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 AWA M 34.00 34.20 34.40 34.60

31641.D GCMS1126.M Fri Feb 01 11:16:56 2002 Page 5

NYC-WTC_000049756

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NYC-WTC_000049756Source: NYC Law Department, mirrored locally

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