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Data File : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial: 6
Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS
Sample ; gc/ms unknown Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 15 Hexatriacontane Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
36.36 1.45 ug/1 148668 Perylene-dl2 37.23
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 507 C36H74 000630-06-8 9K.
2 Heptadecane ’ 240 C17H36 000629-78-7 91 /
3 Tetradecane 198 C14H30 000629-59-4 91 /
4 Heneicosane ___________________________ 296 C21H44 000629-94-7 91/
4bundance Scan 3412 (36.361 min): 23498. D (-) m/z 57.00 100.00%
57
71
43
85
5000
■nfe->
UJ40 (60 80
.,ll,
99
,lil T
100
141 155 169 183
120 140 160 180 200
209
220
239
240 260
281
280
m/z
36.00 36.20 36.40 36'60
71.00 70.94%
Abundance #74636: Hexatriacontane
43 57
71
5000 85
36.00 36.20 36.40 36.60
m/z 43.05 64.74%
97 A
J ' I I' ' ' '1,1 I '
' ' I ' ' ' ' I ' ‘
197 211 _________
I Tt I I I I I I* . . . I I . . I I I . . . ( I I . . I I I . . . I I I I I I . I . . I I >
Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280
4bundance#32063: Heptadecane _ „ .
5/
71
85 36.00 36.20 36.40 36.60
5000 m/z 85.05 51.98%
99
,,,,,,,
Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #69662; Tetradecane I-
---- R Z“71 ->36.00 36.20 36.40 36.60..
m/z 55.00 25.62%
85
5000
■ I ■ ' ■ I I ■ I I ’ I
7 154 198
TA
TlZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 36.00 36.20 36.40 36.60
23498.D NP091101.M Thu Oct 18 10:11:00 2001 Page 15
NYC-Wtc_000088795
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