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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Data File : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial: 6 Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.36 1.45 ug/1 148668 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 9K. 2 Heptadecane ’ 240 C17H36 000629-78-7 91 / 3 Tetradecane 198 C14H30 000629-59-4 91 / 4 Heneicosane ___________________________ 296 C21H44 000629-94-7 91/ 4bundance Scan 3412 (36.361 min): 23498. D (-) m/z 57.00 100.00% 57 71 43 85 5000

■nfe-> UJ40 (60 80 .,ll, 99 ,lil T 100 141 155 169 183 120 140 160 180 200 209 220 239 240 260 281 280 m/z 36.00 36.20 36.40 36'60 71.00 70.94% Abundance #74636: Hexatriacontane 43 57

71 5000 85 36.00 36.20 36.40 36.60 m/z 43.05 64.74% 97 A J ' I I' ' ' '1,1 I ' ' ' I ' ' ' ' I ' ‘ 197 211 _________ I Tt I I I I I I* . . . I I . . I I I . . . ( I I . . I I I . . . I I I I I I . I . . I I > Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 4bundance#32063: Heptadecane _ „ . 5/ 71 85 36.00 36.20 36.40 36.60 5000 m/z 85.05 51.98% 99

,,,,,,, Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #69662; Tetradecane I- ---- R Z“71 ->36.00 36.20 36.40 36.60.. m/z 55.00 25.62% 85 5000

■ I ■ ' ■ I I ■ I I ’ I 7 154 198 TA TlZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 36.00 36.20 36.40 36.60

23498.D NP091101.M Thu Oct 18 10:11:00 2001 Page 15

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NYC-WTC_000088795Source: NYC Law Department, mirrored locally

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