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GC/MS analysis results for sample AD23319, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088450
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23319 .D Vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.49 3.06 ug/1 267430 Perylene-dl2 37.23 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 Abundance Scan 3317 (35.495 min): 23319.D (-) m/z 57.00 100.00% 57

71 43 5000 85 ............ / 99 1 r . J 1, .1,1 ^,J^’',?^’'41155169183197211225239253267281 I , T I , |T> , T I 11 I . i ,, I 1' 1 ,11 1 J ,, 1 I I I 1 I , I I I 1 1 I I 1 I I I I I , I I 35.20 35.40 35.60 35.80 m/z71.00 68.02% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

71 553 85 ..... 35.20 35.40 35.60 35.80 m/z 4^705 60.58% ! J ^J^1?7141155169183197211 I I b I T I I I I I I T I I I I -iTp I I I I I I . I I I .. I I 1 I I I I I' ” • I'"' I'"' I •' •' I '' I' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 5|7 71 H ' ' ' I 85 35.20 35.40 35.60 35.80 553 m/z 85.05 48.54% 99

■n/z-> 40 44 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I'''' I'''' I'''' I 268 I»1111111111 296 f " '' I

Abundance #51002: Heneicosane, ll-(l-ethylpropyl)- 43 57 35.20 35.40 35.60 35.80 m/z 54.95 23.99% 71 5000 85

183197211225 . 338 295 P'' 'I'''' I'''' I' 'I I'' ‘' I'' r ''' r ''' I ‘ 'I r ' 'I " ' ' ' I ' ' Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

23319.D NP091101.M Mon Oct 15 09:49:53 2001 Page 15

NYC-WTC_000088450

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NYC-WTC_000088450Source: NYC Law Department, mirrored locally

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