GCMS analysis comments for sample AD28664, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0401\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octadecane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

34.54 0.44 ug/1 101500 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 /91 2 Pentacosane 352 C25H52 000629-99-2 91 3 Tricosane 324 C23H48 000638-67-51 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 3213 (34:538 min): 28664.D (-) m/ z 57.00 ” 100.00% 57 43 71 85 5000

-41 — , T9+ . n — 1 .lil 113127141155168 183 . 208 240 256 281 34.20 34.40 34.60 34.80 DTTTTTT r ITT Ilf, TTT I it i i p i i ? । .1 I | I I I i | ■ i r ITTTTT r ’ ' 1 ' I...... I " m/z 43.00 78.10% miz-2__ 40__ 60 80 100 120_140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 43 71 85 5000 -+GPRPPPr T91 34.20 34.40 34.60 34.80 __ m/z 71.10 74.10% 22 113127141155 1+r TT‘8 TI"I 224 254 —TTIT"uunuguu miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73718: Pentacosane 43 57 —11 71 34.20 34.40 34.60 34.80 i 5000 : 85 m/ z 85.05 5 7.25%

■ ■ ■ i' — L lli 88 113 127 141 155169183 ................ ............... miz-? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #46165: Tricosane TPPPTT 43 57 34.20 34.40 34.60 34.80 m/z 55.0,0 28.63% 71 5000 85

155169183197211 1' I '1 1 11 IT 99 113127 l| M .1 | r. . . | I . I. f 253 . a| . .i , j . . . . । I . .. । . 297 324 r ■ ■ ■ i ■'1' i1 ■ ■ whA,A —.Z NA ,441 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 34.20 34.40 34.60 34.80

28664.D GCMS1126.M Fri Dec 07 15:54:19 2001 Page 9

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