GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D Vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 35.43 0.90 ug/1 186933 Perylene-dl2 37.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance Scan 3310 (35.428 min): 28430. D (-) m/z 56.95 100.00 57 43 71 85 5000

“I

miz-> LA.2s1F1691e2197211 —.240—2 40 60 80 100 120 140 160 180 200 220 240 ———— m/z43.05 280 300 320 340 260 35.00 35.20 35.40 35.60 35.80 69.96% Abundance #74636: Hexatriacontane 43 57

71 5000 85 35.00 35.20 35.40 35.60 35.80 m/ z 71.00 69.86% 1 0 113127141 155169183197211 " । •11 ■ ’1 . |T. . , I . .T. | . J .'I | | . . . . ( | . . . . | .T ■ | ■ I | ! I > I | I I I I | I I I I | I miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 । 1 11 35.00 35.20 35.40 35.60 35.80 5000 85 m/z 85.05 53.93%

J_। 99 || । j 113127 155169183197 294 338 " I' ■ ■11 ■ —————— i ■ • ■ rI1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane । 14 0 r 57 35.00 35.20 35.40 35.60 35.80 71 m/z 54.95 25.40% 85 5000 99 _745522 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.00 35.20 35.40 35.60 35.80

28430.D GCMS1126.M Wed Dec 05 08:19:58 2001 Page 11

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