GCMS analysis results for sample AD28430, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC0401\28430.D Vial: 12 Acq On : 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Tetratriacontane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 36.29 0.48 ug/1 100020 Perylene-dl2 37.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetratriacontane 479 C34H70 014167-59-0 2 Pentatriacontane 493 C35H72 000630-07-9 87 3 Hexatriacontane 507 C36H74 000630-06-8 87 4 Tetratetracontane 619 C44H90 007098-22-8 87 Abundance Scan 3404 (36.290 min): 28430.D (-) m/z 57.00 100.00% 57

5000 85

“PP= miz-> a0....1’11109,1012002 m/z 71.00 40 60 80 100 120140 160180 200 220 240 260 280 300320 340 360 380400 36.00 36.20 36.40 36.60 69.05% Abundance #58265: Tetratriacontane 57

5000 85 -AAAE-44PPRPM* 36.00 36.20 36.40 36.60 m/z 43.05 60.74%

mlz-> 1 Hi"' 1 44141,169 311 ,।।।।11p।11111■11111111111111111 ■| 40 60 80 100 120140 160180 200 220 240 260 280 300320 340 360 380400 367 410

Abundance #58743: Pentatriacontane 57 T T | ■ I • • 36.00 36.20 36.40 36.60 _ 5000 85 m/z 85.05 44.42%

miz-> ‘ ‘I LL1 113,141 . 169 197 225 i"।" I"।i ‘" ‘i"" i" "i "" i"11111''"I""I "" i”"i""i" ”i 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #74636: Hexatriacontane 57 36.00 36,20 36.40 36,60 m/z 55.00 24.31% 5000

m/z-> 85

| 1113, 141 169 197 "■r" p .1., T..T. ।11.... p i।।।।. 111 j 11 ■ 111 1111111 ■ 11 ■ I TT’TI 11111 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 .. J 36.00 36.20 36.40 36.60

28430.D GCMS1126.M Wed Dec 05 08:20:00 2001 Page 12

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