GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28693.D Vial: 8 Acq On : 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heptacosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 34.54 0.70 ug/1 135652 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qu.

1 Heptacosane 380 C27H56 000593-49-7 91 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Hexatriacontane________________ 507 C36H74 000630-06-8 91 Abundance Scan 3213 (34.539 min): 28693.D (-) m/z 56.95 100.00? 57

85 5000

----- 113 34.20 34.40 34.60 34.80 j , 141 169 191209 239256 whpmpmm ri rr i 11". i m/z 43.05 71.71% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane 57

5000 85 34.20 34.40 34.60 34.80 m/z 71.00 70.13% .... A’l 141 J. 169 196.224 ...... ...... ....... . 380 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #71561: Octadecane 57 +7+4 A-ATPR- PrA 34.20 34.40 34.60 34.80 85 5000 m/ Z 85.05 49.85%

1113141........ 224 254..................... " i" I r | in I | I 111 11 r > 1111 I fH | 111111 H I | I M 1111111 ■: I < |. 1111! I i I p I (! I H 11 p I H I H 11111 mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane 57 34.20 34.40 34.60 34.80 m/z 41.05 27.70% 85 5000

113 11282 “WV n-rp-rr ।. n . jr.. ■ 111t. 111 >. 11111... । > ..I ■ । ।■ 11 > ■ । ■ । < 1111 ■ 1111111 ■ । ■ 1111. ।. 11 । m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 34.20 34.40 34.60 34.80

28693.D GCMS1126.M Thu Dec 06 15:19:52 2001 Page 9

NYC-WTC_000035103