GCMS analysis comments for sample AD28663, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28663 .D vial: 17 Acq On 5 Dec 2001 3:59 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heptadecane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 34.54 0.84 ug/1 167738 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qu.

1 Heptadecane 240 C17H36 000629-78-7 91 2 Hexatriacontane 507 C36H74 000630-06-891 3 Heneicosane 296 C21H44 000629-94-7 90 4 10-Methylnonadecane 282 C20H42 000000-00-0 90 Abundance Scan 3213 (34.537 min): 28663.D (-) m/z 57.00 100.00% 57 43 71

5000 85

TTT—unu

mz-> 11 40 □U + A. i1!. 112127141 155 169182— +210239 ............ 60 80 99

100 120 140 160 180 200 220 240 260 280 300 34.20 34.40 34.60 34.80 m/z 43.00 69.82% Abundance #32063: Heptadecane 57 71 85 5000 TTTFTTTT 34.20 34.40 34.60 34.80 99 m/z71.00 69.53%

m/z-> 40 ■ ■ I • 60 — 80 1’1 . ....................... . 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 5 7 — — .m 71 34.20 34.40 34.60 34.80 5000 85 m/z 85.05 46.20%

97 li Li 113 127 141 155169183197211 . . । T . . . । ■ .1. । । । । I ' ' ' ' I ' ' ' ' I ' mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane —1 1111 L — 1111111 57 34.20 34.40 34.60 34.80 71 m/ z 55.00 27.33%

J 85 5000

99

m/z—> — 40 TUU| 60 +1 113127 141 ‘II , , "T 155 "lT11"TT‘171’ TTITTT"IT .................... 296 111101/0""11128 ‘I1UU8TTT 80 100 120 140 160 180 200 220 240 260 280 300 _ _ 34.20 34.40 34.60 34.80

28663.D GCMS1126.M Thu Dec 06 15:31:40 2001 Page 9

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