GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28692.D Vial: 19 Acq On 5 Dec 2001 5:56 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P. Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 , Heptacosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.53 0.46 ug/1 80956 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptacosane 380 C27H56 000593-49-7 (91 2 Tetratriacontane 479 C34H70 014167-59-0 90 3 Nonadecane 268 C19H40 000629-92-5 90 4 Heneicosane 296 C21H44 000629-94-7 87 Abundance Scan 3212 (34.533 min): 28692.D (-) m/z 56.95 100.00% 57

85 5000

--AA-APPP=/44AAA

nfe-> alde. 207.200....... 40 60 80 100 120140 160180200220240 260 280 300320 340360 380400 34.20 34.40 34.60 34.80 m/z 71.10 87.15% Abundance #52248: Heptacosane 57

5000 85 Mr 4 1 IA—ITTTAAr 34.20 34.40 34.60 34.80 75.15% I I 113 141 . 169 196 224 281 324 380 TTTImu"eTTTTI"I"TTT"T""TTTT"TTT"TTTETUTTT m/z-> 40 60 80 100120140160180200 220240 260 280 300 320 340 360 380400 Abundance #58265: Tetratriacontane 57

34.20 34.40 34.60 34.80 5000 85 m/z 85.05 56.49%

114141,169, 11"1■11 ■1 ■ I"'' l'1'11 311 TTTTTT 367 410 mlz-> Abundance 40 60 80 100120140160180200 220 240 260 280 300 320340 360 380400 57 #37469: Nonadecane A A ' 'l 1 1 1 ’ | 1 L 34.20 34.40 34.60 34.80 m/z 55.00 30.69% 85 5000

’" I 1' J.l 183 268 AMM MYWW m/z—> 40 60 80 100120140160180200 220 240260 280 300 320 340 360 380 400 34.20 34.40 34.60 34.80

28692.D GCMS1126.M Thu Dec 06 12:39:44 2001 Page 10

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