GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28692.D vial: 19 Acq On 5 Dec 2001 5:56 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Triacontane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 35.42 0.42 ug/1 58048 Perylene-dl2 37.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 6 2 10-Methylnonadecane 282 C20H42 000000-00-0 3 Heptacosane 380 C27H56 000593-49-7 80

u 4 Dotriacontane 451 C32H66 000544-85-4 80 Abundance Scan 3309 (35.423 min): 28692.0 (-) m/ z 57.00 100.00% 57

85 5000 MMMAP A 113 141 197 35.00 35 20 35.40 35 60 35.80 1 H | I I I I | I I 11 | I 11 I 11 11 I | i > 11 11 i I i 11 | TTTTTTI’TT I’TT I | II I I | 11 I I 11 I I 11 I I I l| 111 m/z 43.00” 74.67% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #55461: Triacontane 43 71 5000 Mowy MA 35.00 35.20 35.40 35.60 35.80 m/z 71.10 63.25%

m/z~> 111 n1 11.2127+... 239 267 TWTTTTTTT) TT 379 422 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #39858:10-Methylnonadecane 57

35.00 35.20 35.40 35.60 35.80 85 m/ Z 85.05 53.54%

J.. 5000

154

mz-> Lm 113 i ■ ■" । । । । । ■■■■।‘।.... ।।। TTOUu 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74082: Heptacosane TTLC—T11—TT ri ‘ 11151111 43 35.00 35.20 35.40 35.60 35.80 m/z 55.00 34.33%

N 71 t$

5000

m/z—> TnTTUto 183 211 TTTggTT 253 353 380 40 60 80 100120140160180200220240260280300320340360 380400420 4 WAAAMA IWCMMMAL 35.00 35.20 35.40 35.60 35.80

28692.D GCMS1126.M Thu Dec 06 12:39:46 2001 Page 11

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