GCMS unknown compounds report, sample AD31253, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0802\31253.D Vial: 10 Acq On 9 Jan 2002 10:34 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Triacontane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

36.12 0.46 ug/1 72312 Perylene-d12 36.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Eicosane, 9-octyl- 4 Dotriagontane S 394 C28H58 451 C32H66 013475-77-9 000544-85-4 90 90 Abundance 7............... Scan 3385 (36.118 mln): 31253.D (-) m/ z 57

5000 85

■ • i • • T

m/z-> Alad’1428. 50 100 150 200 281 250 300 350 400 450 500 550 600 35.80 36.00 36.20 36.40 m/z 43.00 81.50% Abundance #55461: Triacontane 433 71 5000 35.80 36.00 36.20 36.40 ' m/z 71.10 68.00% 11 I; 99 127 .. 11111111 239267 379 422 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance 461 068: Tetraletracontone 57 •11 • • > ■ । ■ • ■ ■ । ■ * ■11 ■ ’' ■ । 35.80 36.00 36.20 36.40 5000 85 m/z 85.05 47.13%

113141169197225 379407 590618 m/z-> &o' 100 150 200 250 " 300 350 400 450 5001 550 600 Abundance #53460: Eicosane, 9-octyl- A AAA ■ .A । 43 35.80 36.00 36.20 36.40 71 m/z 55.00 25.32% 5000

m/z-> ■ I’ 50 —99,127155 Hr 238 __ 281 — ........ 352 394........................................... 100 150 200 250 300 350 400 450 500 550 600 -Aw MMMay 35.80 36.00 36.20 36.40

31253.D GCMS0103.M Wed Feb 06 11:21:40 2002 Page 5

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