NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\JAN0802\31253.D Vial: 10
Acq On 9 Jan 2002 10:34 pm Operator: 209 GALOS
Sample gems scan 12/24 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 5
R.T. EstConc. Area Relative to ISTD R.T.
14.17 0.23 ug/1 79651 Naphthalene-d8 15.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74
2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 47
3 3,4 -Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 43
4 Benzoic acid, 2. -bis[(trimethylsil 370 C16H3004Si3 003782-85-2 33
Abundance Scan 994 (14.168 mtn): 31253.D (-) m/ z 73.0,0 100.00%
73
5000
267
355
45 13.80 14.00 14.20 14.40
, 103 133 154. 177 193 . 223 251 1 Mr 11fi rrr
—"Immmegu —upaummnanur 111111323339 m/z 267.00 32.16%
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000 ‘iR T 18
13.80 14.00 14.20 14,40
m/z 355.0 22.69%
191207 251 323339
. I ....jI .... j .... 1 . I .. 1 .... 1 .... 1 .... 1 .... 1.T..1 .... 1 . . 1' TT »»V‘ > * “ i ■ * *11
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance 572978: Benzene acid 2.3-butbmemyisoy) trmothyls
73
355 ..... . .............
13.80 14.00 14.20 14.40
5000- m/z 74.00 8.91%
45
147 179 207223 267282297 370
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)-
73 13.80 14.00 14.20 14.40
m/z 356.0 8.34%
5000 267
179
356
45 147
|, , 209 237
'I nyi i i'i 111 > 11 > i n 11 TTI—Tmupg)" ‘ > I»“ ‘ J ‘312 341
‘ “ I “ ‘ ’ r' ‘ n TTTp
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40
31253.D GCMS0103.M Wed Feb 06 11:21:36 2002 Page 4
NYC-WTC_000016452
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