Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.
NYC-WTC_000018123–000018141Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank II
R.T. EstConc Area Relative to ISTD R.T.
14.30 0.34 ug/1 102757 Naphthalene-d8 15.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
I Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4 -Dihydrox benzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 4 Benzoic acid. 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 35 Abundance C Scan 1009 (14.305 mln): 30696.D (-) m/z 73.00 100.00% 73
5000 267 355 T TTnuami 45 , i 125 154 177 193 223 251 h 14.00 14.20 14.40 14.60 323339 1 - T2—mmg*m—an*d*n—m—mmTTTETHpu’ . ‘ i."' i'. ‘1 '1 “1 “i' ‘ ' i m/z 266.90 32.32% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 733 355 267 5000 T T T T 1 14.00 14.20 14.40 14.60 m/z 355.0 22.33% 191207 251 323339 | ।. i M 111111।।, 11.11. i. ।।।|।. • ■ i ■ ■ “ i1 ■ ■ ■ I ■1 • 'i ‘ i • ■" i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bis(trimethylsilaxy)- trimethyls 73 355 14.00 14.20 14.40 14.60 ‘ ‘ 5000 m/z 74.00 9.82% 45 147 267282297 370 . .•!.... । . . ..!....।....।....।... . 179 207223 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3.4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.00 14.20 14.40 14.60 m/z 356.05 9.05% 267 5000 179 356 45 147 I. , . » J i f 17 | TT T1 pFi i । i i i > I . I . H if. » I . , 209 237 , ICWwmarpage 312 341 I rl •1 “ i v-tt-j-t T-r-j-r-r-r-r-) m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30696.D GCMS1126.M Wed Jan 23 08:36:47 2002 Page 4
NYC-WTC_000018133
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NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049745
GCMS analysis report for sample AD31641 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036513
Laboratory commentary noting low recovery and acidic pH for sample AD29187, recommending re-extraction and re-analysis on January 4, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder