GCMS analysis log for sample AD30696, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3 101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***************************************************************** ** * * Peak Number 5 Heptadecane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

33.60 0.35 ug/1 70652 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecahe . x 240 C17H36 000629-78-7 93 2 Nonacosane A4 * 408 C29H60 000630-03-5 90 3 Hexatriacontane 1o 507 C36H74 000630-06-8 87 4 Eicosane 282 C20H42 000112-95-8 86 Abundance 57 Scan 3111 (33.602 mln): 30696.D (-) m/ z 57.00 100.00%

5000 85

3w 44129/ -p-T 33.20 33.40 33.60 33.80 34.00 m/z 43.00 72.03% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #71193: Heptadecane 57

5000 85 33.20 33.40 33.60 33.80 34.00 m/z 71.05 59.10% TTrp-rr , 113,141 । r. i 169 f. ।.... f.।।।। 210 240 ।।।।।i. 1111111 > 11111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526. Nonacosane 43 AAA M, ,, , , Al , J t M IA 71 33.20 33.40 33.60 33.80 34.00 5000 m/z 42.17%

- I 199 127 211 239 379 408 t...,,।।(.........।.........j.... ].... ।.... । m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 Abundance 57 #74635: Hexatriacontane -AM-— IA 33.20 33.40 33.60 33.80 34.00 m/z 41.05 36.68% 5000 85

mm I u 113,141 , 196 225 253 281 TqTk • 111 tli 1111 > । > । > 1111 > 1111 h 111111111 • । • 111 j । > 11 p 11111 > । > 11 > 111111 > । > 11111 j i j 111111 wW A WWW miz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 33.20 33.40 33'60 33.80 34.00

30696.D GCMS1126.M Wed Jan 23 08:36:52 2002 Page 5

NYC-WTC_000018134