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GCMS analysis log for sample AD30696, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.

NYC-WTC_000018123–000018141

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018135
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30696.D Vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Hexatriacontane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.52 0.62 ug/1 124598 Chrysene-dl2 33.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Dotriacontane 451 C32H66 000544-85-4 91 4 Nonacosane 408 C29H60 000630-03-5 91 Abundance Scan 3211 (34.520 mln): 30696.D (-) m/ Z 57.00 100.00% 57

5000 85

"BI • • 1 ‘ ■ r • r

m/z—> +4420240,21— 50 100 150 200 250 300 350 400 450 500 550 600 34.20 34.40 34.60 34.80 m/z 43.00 81.44% Abundance #74636: Hexatriacontane 57

5000 85 Tm 1**) 34.20 34.40 34.60 34.80 m/z 71.0A0 64.53% I 1113141 169 197 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontanc ! 57 PM121 1“ ! 11TPArm 34.20 34.40 34.60 34.80 5000 85 m/z 85.05 45.68%

i 113141 169 197225 .... ....... ...................... . miz-> 50 100 150 200 250 300 350 400 450 500 550 ‘ 600 ‘ ' Abundance #74490: Dotriacontane - MAPAAAAt 43 34.20 34.40 34.60 34.80 m/z 41.05 30.90% 71 5000

j| 18,127155183 .... 379407 .450 ............................... m/z-> 50 100. 150 200 250 300 350 400 450 500 550 ‘ 600 34.20 34.40 34.60 34.80

30696.D GCMS1126.M Wed Jan 23 08:36:57 2002 Page 6

NYC-WTC_000018135

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NYC-WTC_000018135Source: NYC Law Department, mirrored locally

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