GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0401\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

32.66 1.10 ug/1 239005 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-894 2 Pentacosane 352 C25H52 000629-99-2 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Dotriacontane 451 C32H66 _______ 000544-85-4 91 Abundance Scan 3008 (32.856 min): 28677.D (-) m/z 57.00 100.00% 57

5000 85

rm TTT—r IT . TTmuur J , 13141169197225 267 32.40 32.60 32.80 33.00 TTrTTTTTTTinTtuufuTrumTTTTPTTTTTTTTT m/z 43.05 69.45%

1 miz-x 50!100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 5fr

5000 TTTT ' T i ■ 1 85 32.40 32.60 32.80 33.00 m/z 71.00 66.90%

miz-> ' ' I ' 50 113141169197 100 ............ 150 200 250 300 350 400 450 500 550 600 Abundance #73713: Pentacosane 43 1 : ——————— 71 32.40 32.60 32.80 33.00 5000 m/ z 85.0, 46.58%

. L i 92 127155 183211 ...................... ................... miz- 50 100 150 200 250 300 ' 350 400 450 ' 500 550 600 Abundance #61068: T etratetracontane TT TTr TTn—rr 57 32.40 32.60 32.80 33.00 m/z 41.00 30.00% 5000 85

113141169 197225 P T‘ I T TT , | , , ■ . | H b ‘ p 379407 590618 "PMMPP • • i • ' ' ' I ' ' • ' I ' ' ' ' I * 1 '1 I ' ' • ' p ' -j-r miz-> 50 100 150 200 250 300 350 400 450 500 550 600 32.40 32.60 32.80 33.00

28677.D GCMS1126.M Fri Dec 07 15:12:15 2001 Page 7

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