GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 01\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Tetracosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.66 1.55 ug/1 338679 Chrysene-dl2 33.03

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Tetracosane 338 C24H50 000646-31-1 94 2 Octadecane 254 C18H38 000593-45-3 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Nonadecane, 2-methyl- 282 C20H42 _______ 001560-86-7 91 Abundance Scan 2900 (31.665 min): 28677.D (-) m/z 57.00 100.00% 57 43 71 85 5000 TIPTPTP 99 144 31.40 31.60 31.80 32.00 0 T’il 4,4,1,147111155169183197211225239253267281 338 111111111111111 m/z 43.. 05 71.14% miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 H ! 71 5000 85 T 1 1. 1 1 31.40 31.60 31.80 32.00 99... m/z 71.00 69.86% ' l« »' *1 •' TIT 1 113127 TTTTTTTTTTTTTTT 155169183197 294 p-rrs-rm rp-n-r-p-m-j- 338 i1 • ■11 i ■ ■ • ■ i • ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 43 7i - - -P 31.40 31.60 31.80 32.00 ' 85 m/z 85.05

.A 5000 50.49%

Is! 99 113127141155 "I1' "I"1 • ■ i ■ F : i r ■ ■' r '1111''11 i ■ • • ■ i 224 Iu 254 ——TT i " " i ■ " 111" ' I ■ ■ miz—? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane k r ' ' I 1 । r । | । । rr | ■ ■ i ' ■ 43 57 31.40 31.60 31.80 32.00 71 m/z 41.05 28.64% । 5000 85

99 113127141155 196 240 282 m/z-> JJ ‘ I | rrit | TTTTTIPT] , , TT-rm-j-n -------------------- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

28677.D GCMS1126.M Fri Dec 07 15:12:10 2001 Page 6

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