GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28694.D vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.54 0.43 ug/1 106550 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# 93 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetratetracontane 619 C44H90 007098-22-8191 3 Heptadecane 240 C17H36 000629-78-7 91 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 3213 (34.538 min): 28694.D (-) m/z 57.00 100.00% 57

85 5000-

f ‘ i1

miz-> h 50 114 100 150 209 256 TIPI——m—*mTTITT 200 250 300 350 400 450 500 550 CT) 34.20 34.40 34.60 34.80 m/z71.10 77.08% Abundance #74636: Hexatriacontane 57

5000 +PPA-T-NP. 85 34.20 34.40 34.60 34.80 m/z 43.00 71.58%

mlz-> Abundance

5000 ' ■ ■ i1 50 57

85 113141169197 A..... . । । . . .... .......... — 100 150 200 250 300 350 400 450 500 550 600 #74745: Tetratetracontane

1 1 1 1 1 • • i « • • < I 34.20 34.40 34.60 34.80 m/z 85.05 53.67%

, 11341 —....... . ................................... 463491519547,591618 ' b 1 i 1 mz-> 50 100 150 200 250 300 350 400 450 500 550 ' 600 Abundance #71193: Heptadecane 1 ' 1 1 1 4441A 57 34.20 34.40 34.60 34.80 m/z55.00 30.03%

5000 85

' 1 i ■ 1100 113141169 210240 —..... ............................ AAGMAAAH MYMA m/z—> 50 150 200 250 300 350 400 450 500 550 600 34.20 34.40 34.60 34.80

28694.D GCMS1126.M Thu Dec 06 15:34:15 2001 Page 9

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