GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC04 01\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heptadecane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 35.43 0.41 ug/1 82976 Perylene-dl2 37.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 2 Pentacosane 352 C25H52 000629-99-2 3 Heptacosane 380 C27H56 000593-49-7 91 4 Hexatriacontane_________ _______________ 507 C36H74 000630-06-8 91 Abundance Scan 3310 (35.428 min): 28694.D (-) m/z 57.00 100.00% 57

5000 85

4 35.00 35.20 35.40 35.60 35.80

mlz-> T L 113,141 169 191207 240 TTTTuTTTTTTT ’TTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 111111 m/z 71.00 74.32% Abundance #71193: Heptadecane 57

5000 T‘ TIuT—DTT——rruuu 85 35.00 35.20 35.40 35.60 35.80 m/z 43.05 73.20% , j 113 , 141 169 210 240 " ■ I" I’T mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #73718: Pentacosane 43 .... — 35.00 35.20 35.40 35.60 35.80 71 5000 m/z 85.05 46.98%

miz-> Abundance " ■ i"' J 11" 11 QQ 7,127 155 183 ITT—0‘r0""ICOTTITTTTIT 211 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 57 #52248: Heptacosane -M+4-A—A AA 1 35.00 35.20 35.40 35.60 35.80 m/z 54.95 25.56% 5000 85

l i 1113 141 . 169 196 224 281 324 380 TTITTTTTETTgau TTTT—TT m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 35.00 35.20 35.40 35.60 35.80

28694.D GCMS1126.M Thu Dec 06 15:34:17 2001 Page 10

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