GCMS blank analysis for sample AD28662, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC04 01\28662.D Vial: 15 Acq On 5 Dec 2001 2:02 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heptacosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 35.42 0.42 ug/1 69644 Perylene-dl2 37.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 87) 2 Pentatriacontane 493 C35H72 000630-07-9 87 3 Hexatriacontane 507 C36H74 000630-06-8 87 4 Tetratetracontane 619 C44H90 007098-22-8 87 Abundance Scan 3309 (35.422 min): 28662.D (-) m/z 57.00 100.00% 57

5000 85 4'

• i MAPP • । 35.00 35.20 35.40 35.60 35.80 113,141 . 191207 TTTTTTTTTTTTTTTTpr m/z 71.00 72.14% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane 57

5000 CYM MA A 11 — I — l --- 85 35.00 35.20 35.40 35.60 35.80 m/z 43.05 63.47% ...... ..... ................................................................. ............ ................ .. miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #58743: Pentatriacontane 57 AM AAAP . 7177 A AA A4 35 00 35.20 35.40 35.60 35.80 5000 85 m/z 85.05 43.21%

| | || 113,141 169 197 225 "I" n. । t v. ।। ।j।।।।।ji’ 11111111 j > । tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74635: Hexatriacontane . A . A __ i i • ■ ' ■ i I ‘ 1 T i 1 ■ 57 35.00 35.20 35.40 35.60 35.80 m/z 41.05 29.13%

5000 85

m/z—> LL 113 141 196 225 253 281 — TTTICTITTTTTTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 MADMMr, AAn 35.00 35.20 35.40 35.60 35.80

28662.D GCMS1126.M Thu Dec 06 13:20:21 2001 Page 10

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