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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088131
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23262.D Vial: 8 Acq On 9 Oct 2001 8:12 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Heptacosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.36 0.45 ug/1 76740 Perylene-dl2 37.24 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

Heptacosane 380 C27H56 000593-49-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 87 3 Tetratriacontane 479 C34H70 014167-59-0 87 4 Tritetracontane 605 C43H88 007098-21-7 86 Abundance Scan 3412 (36.363 min): 23262.D (-) m/z 57.00 100.00% 57

85 5000-

36.00 36.20 36.40 36.60 Wz 71.00 83.98% TTfe-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #52248: Heptacosane 57

5000 85 ‘ ' ''' ' 1'7'’ ' '"IQ 36.00 36.20 36.40 36.60 m/z 47705 63792% 281 324 380 " ' I" ' p-OTYnT-qTT¥T7TVTTfTTTVp-rTTpTrtT1TTr|^^ " i"'' I' ‘' I " ‘' I" " I' "' I"' ‘ I" " I tVz-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #74636: Hexatriacontane 57 I ■ 36,00 36,20 36.40 36.60 85 m/z 85.05 54.44% li

I I II . 169 197 n/z-> Abundance I < > 11171.111 J I:. JI.. 11,11111... 11. <. I... 11.... I,. 111.11111 MIP >.. I.... 11.. 11

40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400

57 #58265: Tetratriacontane I K 36.00 36.20 36.40 36.60 A

"m/z 55.00 30.99%

5000- 85

311 367 410 -m-p-TT I I II r I f l I I I I i7i I I I I I (I I 11 j I I I I I"'' I" " I" " I" " I I'"' I" " I I' "' I"'' I' " ‘ I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 36.00 36.20 36.40 36.60

23262.D NP091101.M Thu Oct 11 10:48:15 2001 Page 10

NYC-WfC_000088i31

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NYC-WTC_000088131Source: NYC Law Department, mirrored locally

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